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  1. Home
  2. Air Emission Measurement Center (EMC)
  3. Technical Support

EMC Methods Support Directory

Alternative Test Methods Determinations

  • Kim Garnett             919/541-1158 – Primary

Protocol Calibration Gas Questions

  • Donna Nolen-Weathington 919/541-7525 - Primary
  • Walter Lin                 919/541-1341 - Backup

    SPS Method (40 CFR Part 60, Appendix A)

    General Provisions 

    • Kim Garnett             919/541-1158 – Primary
    • Hannah Halliday         919/541-2431 - Backup

    Method 1 (Traverse Points)

    • Walter Lin                919/541-1341 - Primary
    • Mike Toney             919/541-5247 - Backup

    Method 1A (Traverse points in small ducts)

    • Walter Lin                 919/541-1341 - Primary
    • Mike Toney             919/541-5247 - Backup

    Method 2 (Velocity - S type pitot)

    • Walter Lin                 919/541-1341 - Primary
    • Mike Toney             919/541-5247 - Backup

    Method 2A (Flow rate in small ducts - volume meters)

    • Walter Lin                 919/541-1341 - Primary
    • Mike Toney             919/541-5247 - Backup

    Method 2B (Low flow rate - stoichiometry)

    • Walter Lin                 919/541-1341 - Primary
    • Mike Toney             919/541-5247 - Backup

    Method 2C (Flow rate in small ducts - standard pitot)

    • Walter Lin                 919/541-1341 - Primary
    • Mike Toney             919/541-5247 - Backup

    Method 2D (Flow rate in small ducts - rate meters)

    • Walter Lin                 919/541-1341 - Primary
    • Mike Toney             919/541-5247 - Backup

    Method 2E (Landfill gas production flow rate)

    • Walter Lin                 919/541-1341 - Primary

    Method 2F (3-D Pitot)

    • Walter Lin                 919/541-1341 - Primary

    Method 2G (Determination of Stack Gas Velocity and Volumetric Flow Rate With Two-Dimensional Probes)

    • Walter Lin                919/541-1341 - Primary

    Method 2H (Determination of Stack Gas Velocity Taking Into Account Velocity Decay Near the Stack Wall)

    • Walter Lin                919/541-1341 - Primary

    Method 3 (Molecular weight of stack gases)

    • Walter Lin                919/541-1341 - Primary
    • Ned Shappley        919/541- 7903 – Backup

    Method 3A (Carbon dioxide (CO2), Oxygen (O2) - inst.)

    • Walter Lin                919/541-1341 – Primary
    • Kim Garnett             919/541-1158 - Backup  

    Method 3B (CO2, O2 - Orsat)

    • Walter Lin                919/541-1341 - Primary
    • Ned Shappley        919/541- 7903 – Backup

    Method 3C (CO2, CH4, N2, and O2)

    • Donna Nolen-Weathington 919/541-7525 - Primary
    • Walter Lin                919/541-1341 - Backup

    Method 4 (Moisture content)

    • Walter Lin                919/541-1341 - Primary

    Method 5 (Particulate matter (PM))

    • Walter Lin                  919/541-1341 - Primary
    • Paul Van Rooy                919-541-4464-Backup

    Method 5A (PM - asphalt roofing)

    • Walter Lin                  919/541-1341 - Primary

    Method 5B (PM - nonsulfuric acid)

    • Walter Lin                  919/541-1341 - Primary

    Method 5D (PM - baghouses)

    • Walter Lin                 919/541-1341 – Primary
    • Ned Shappley        919/541- 7903 – Backup

    Method 5E (PM -fiberglass plants)

    • Walter Lin                  919/541-1341 - Primary

    Method 5F (PM - fluid catalytic cracking unit)

    • Walter Lin                  919/541-1341 - Primary

    Method 5G (PM - wood stove - dilution tunnel)

    • Mike Toney             919/541-5247 - Primary

    Method 5H (PM- wood stove - stack)

    • Mike Toney             919/541-5247 - Primary

    Method 5I (Low Level Particulate Matter Emissions)

    • Walter Lin                  919/541-1341 - Primary

    Method 6 (Sulfur dioxide (SO2)

    • Ned Shappley        919/541- 7903 - Primary

    Method 6A (SO2, CO2)

    • Ned Shappley        919/541- 7903 - Primary

    Method 6B (SO2, CO2 - long term integrated)

    • Ned Shappley        919/541- 7903 - Primary

    Method 6C (SO2 - instrumental)

    • Walter Lin                919/541-1341 – Primary
    • Kim Garnett             919/541-1158 - Backup 

    Method 7 (Nitrogen oxide (NOX))

    • David Berkowitz     919-541-4767 – Primary
    • Donna Nolen-Weathington 919/541-7525 - Backup

    Method 7A (NOX - ion chromatographic method)

    • Dave Nash             919/541-9425 - Primary

    Method 7B (NOX - ultraviolet spectrophotometry)

    • David Berkowitz     919-541-4767 – Primary
    • Donna Nolen-Weathington 919/541-7525 - Backup

    Method 7C NOX - Alkaline-permanganate/colorimetric)

    • David Berkowitz     919-541-4767 – Primary
    • Donna Nolen-Weathington 919/541-7525 - Backup

    Method 7D (NOX - alkaline-KMNO4/ion chromatographic)

    • David Berkowitz     919-541-4767 – Primary
    • Donna Nolen-Weathington 919/541-7525 - Backup

    Method 7E (NOX - instrumental analyzer procedure)

    • Walter Lin                919/541-1341 – Primary
    • Kim Garnett             919/541-1158 - Backup 

    Method 8 (Sulfuric acid mist and SO2)

    • Ned Shappley        919/541- 7903 – Primary
    • Paul Van Rooy                919-541-4464-Backup

    Method 9 (Opacity)

    • Kim Garnett           919/541-1158 - Primary

    Method 10 (Carbon monoxide (CO) - NDIR)

    • Walter Lin                919/541-1341 – Primary
    • Kim Garnett             919/541-1158 - Backup 

    Method 10A (Carbon monoxide (CO) - colorimetric )

    • Ned Shappley        919/541- 7903 - Primary

    Method 10B (Carbon monoxide - GC)

    • Ned Shappley        919/541- 7903 - Primary

    Method 11 (H2S)

    • David Berkowitz     919-541-4767 – Primary

    Method 12 (Lead - atomic absorption)

    • Kim Garnett             919/541-1158 - Primary

    Method 13A (Total fluoride - colorimetric)

    • David Berkowitz     919-541-4767 – Primary
    • Ned Shappley        919/541- 7903 - Backup

    Method 13B (Total fluoride - specific ion electrode)

    • David Berkowitz     919-541-4767 – Primary
    • Ned Shappley        919/541- 7903 - Backup

    Method 14 (Fluoride - potroom roof monitors)

    • David Berkowitz     919-541-4767 – Primary
    • Ned Shappley        919/541- 7903 - Backup

    Method 14A (Total Fluoride – Primary Aluminum)

    • David Berkowitz     919-541-4767 – Primary
    • Ned Shappley        919/541- 7903 - Backup

    Method 15 (TRS petroleum refineries)

    • David Berkowitz     919-541-4767 – Primary

    Method 15A (TRS - oxidation/Method 6)

    • David Berkowitz     919-541-4767 – Primary

    Method 16 (TRS - kraft pulp mills)

    • David Berkowitz     919-541-4767 – Primary

    Method 16A (TRS - oxidation/Method 6)

    • David Berkowitz     919-541-4767 – Primary

    Method 16B (TRS - oxidation/GC)

    • David Berkowitz     919-541-4767 – Primary

    Method 16C (TRS - Real Time Data)

    • Kim Garnett           919/541-1158   - Primary
    • David Berkowitz     919-541-4767 – Backup

    Method 17 (Particulate - in-stack filtration method)  

    • Walter Lin                  919/541-1341   - Primary

    Method 18 (VOC - gas chromatography)

    • Ned Shappley          919/541- 7903 - Primary
    • David Berkowitz     919-541-4767 – Backup

    Method 19 (Calculation procedure - power plants)

    • Donna Nolen-Weathington919/541-7525 - Primary
    • Kim Garnett          919/541-1158   - Backup

    Method 20 (NOX - gas turbines)

    • Kim Garnett           919/541-1158   - Primary

    Method 21 (Volatile organic compounds (VOC) leaks)

    • Ned Shappley        919/541- 7903 – Primary
    • Walter Lin                  919/541-1341 - Backup

    Method 22 (Visual determination of fugitive emissions)

    • Kim Garnett           919/541-1158   - Primary

    Method 23 (Dioxin and Furans)

    • Ned Shappley        919/541- 7903 –Primary

    Method 24 (VOC - solvent in surface coatings)

    • Ned Shappley        919/541- 7903 – Primary
    • Donna Nolen-Weathington  919/541-7525 - Backup

    Method 24A (VOC - solvents in ink)             

    • Ned Shappley        919/541- 7903 – Primary
    • Donna Nolen-Weathington  919/541-7525 - Backup

    Method 25 (TGNMO - oxidation/reduction)

    • Donna Nolen-Weathington  919/541-7525 - Primary

    Method 25A (TOC - FID)

    • Ned Shappley        919/541-7903 - Primary

    Method 25B (TOC - NDIR)

    • Ned Shappley        919/541-7903 - Primary

    Method 25C (Nonmethane organic compounds in landfills)

    • Donna Nolen-Weathington 919/541-7525 - Primary

    Method 25D (Volatile organics from waste samples)

    • Ned Shappley        919/541-7903 –Primary

    Method 25E (Vapor phase organics in waste samples)

    • Ned Shappley        919/541-7903 - Primary

    Method 26 (HCl)

    • Ned Shappley             919/541-7903 - Primary

    Method 26A (HCl)

    • Ned Shappley             919/541-7903 – Primary
    • Paul Van Rooy                919-541-4464-Backup

    Method 27 (VOC - leaks/tank trucks)

    • Dave Nash                   919/541-9425 – Primary
    • Walter Lin                  919/541-1341 - Backup

    Method 28 (Wood stove certification)

    • Mike Toney               919/541-5247 - Primary

    Method 28A (Air to fuel ratio)

    • Mike Toney               919/541-5247 - Primary

    Method 28R (Certification and Auditing of Wood Heaters)

    • Mike Toney               919/541-5247 - Primary

    Method 28 WWH (Particulate Emissions and Heating Efficiency of Hydronic Heaters)

    • Mike Toney               919/541-5247 - Primary

    Method 28 WWH PTS (Cord Wood-Fired Hydronic Heaters: Partial Thermal Storage)

    • Mike Toney               919/541-5247 - Primary

    Method 29 (Multiple Metals)

    • Kim Garnett           919/541-1158   - Primary

    Method 30A (Mercury Instrumental)

    • Ned Shappley          919/541-7903 – Primary

    Method 30B (Mercury Sorbent Trap)

    • Ned Shappley          919/541-7903 – Primary

    Top of Page

    NESHAP Methods (40 CFR Part 61, Appendix B)

    Method 101 (Mercury - air streams)

    • Ned Shappley            919/541-7903 - Primary

    Method 101A (Mercury - sewage sludge incinerators)

    • Ned Shappley            919/541-7903 - Primary

    Method 102 (Mercury - hydrogen streams)

    • Ned Shappley            919/541-7903 - Primary

    Method 103 (Beryllium screening method)

    • Kim Garnett             919/541-1158 - Primary

    Method 104 (Beryllium)

    • Kim Garnett             919/541-1158 - Primary

    Method 105 (Mercury - sewage sludge)

    • Ned Shappley            919/541-7903 - Primary

    Method 106 (Vinyl Chloride)

    • David Berkowitz     919-541-4767 – Primary
    • Ned Shappley          919/541-7903 – Backup

    Method 107 (Vinyl Chloride - process streams)

    • David Berkowitz     919-541-4767 – Primary
    • Ned Shappley          919/541-7903 – Backup

    Method 107A (Vinyl Chloride - process streams)

    • David Berkowitz     919-541-4767 – Primary
    • Ned Shappley          919/541-7903 – Backup

    Method 108 (Inorganic arsenic)

    • Dave Nash                   919/541-9425 – Primary

    Method 108A (Arsenic - ore samples)

    • Dave Nash                   919/541-9425 – Primary

    Method 108B (Arsenic - ore samples)

    • Dave Nash                   919/541-9425 – Primary

    Method 108C (Arsenic - ore samples)

    • Dave Nash                   919/541-9425 – Primary

    Method 111 (Polonium 210)

    • Jonathan Walsh      202/343-9238 - Primary

    Method 114 (Radionuclide)

    • Jonathan Walsh      202/343-9238 - Primary

    Method 115 (Radon)

    • Jonathan Walsh      202/343-9238 - Primary

    Top of Page

    SIP Methods (40 CFR Part 51 Appendix M)

    Method 201 (PM10 (EGR procedure))

    • Ned Shappley             919/541-7903 – Primary
    • Dave Nash                   919/541-9425 - Backup

    Method 201A (PM10 (CSR procedure))

    • Ned Shappley             919/541-7903 – Primary
    • Dave Nash                   919/541-9425 - Backup

    Method 202 (Condensible PM)

    • Dave Nash                   919/541-9425 - Primary
    • Ned Shappley             919/541-7903 - Backup

    Method 203A (Opacity)

    • Ned Shappley             919/541-7903 - Primary

    Method 203B (Opacity - time exception)

    • Ned Shappley             919/541-7903 - Primary

    Method 203C (Opacity - Installments)

    • Ned Shappley             919/541-7903 - Primary

    Method 204 (VOC Capture Efficiency)

    • Ned Shappley             919/541-7903 - Primary

    Method 204A (VOC Capture Efficiency)

    • Ned Shappley             919/541-7903 - Primary

    Method 204B (VOC Capture Efficiency)

    • Ned Shappley             919/541-7903 - Primary

    Method 204C (VOC Capture Efficiency)

    • Ned Shappley             919/541-7903 - Primary

    Method 204D (VOC Capture Efficiency)

    • Ned Shappley             919/541-7903 - Primary

    Method 204E (VOC Capture Efficiency)

    • Ned Shappley             919/541-7903 - Primary

    Method 204F (VOC Capture Efficiency)

    • Ned Shappley             919/541-7903 - Primary

    Method 205 (Calibration Gas Dilution)

    • Ned Shappley            919/541-7903 - Primary
    • Walter Lin                  919/541-1341 - Backup

    Method 206 (Ammonia) ** Method 206 has been renamed to Conditional Test Method (CTM) 027

    • Dave Nash                   919/541-9425 – Primary

    Method 207 (Corn Wet-Milling Presurvey)

    • David Berkowitz     919-541-4767 – Primary
    • Ned Shappley          919/541-7903 – Backup

    Top of Page

    MACT Methods (40 CFR Part 63 Appendix A)

    Method 301 (Test Data Validation)

    • Paul Van Rooy                919-541-4464 - Primary
    • Hannah Halliday         919/541-2431 - Backup

    Method 302 (General GC/MS) METHOD CANCELLED

    Method 303, 303A (Coke Oven Emissions)

    • Kim Garnett                 919/541-1158 - Backup
    • Ned Shappley             919/541-7903 - Primary

    Method 304A, 304B (Biodegradation rate)

    • Ned Shappley             919/541-7903 – Primary
    • Donna Nolen-Weathington 919/541-7525 - Backup

    Method 305 (Compound specific liquid waste)

    • Ned Shappley             919/541-7903 - Primary
    • Donna Nolen-Weathington919/541-7525 - Backup

    Method 306 (Hexavalent Chromium)

    • David Berkowitz     919-541-4767 – Primary

    Method 306A (Simplified Chromium Sampling)

    • David Berkowitz     919-541-4767 – Primary

    Method 306B (Surface Tension for Tanks Electroplating and Anodizing)

    • David Berkowitz     919-541-4767 – Primary

    Method 307 (Solvent Degreaser VOC)

    • David Berkowitz     919-541-4767 – Primary
    • Ned Shappley             919/541-7903 - Backup

    Method 308 (Methanol)

    • David Berkowitz     919-541-4767 – Primary
    • Ned Shappley             919/541-7903 - Backup

    Method 310A, B, C (Hexane in EPDM Rubber)
    Industry developed methods.  EMC does not provide technical support.

    Method 311 (VOC HAPs in furniture coatings)

    • Ned Shappley             919/541-7903 - Primary

    Method 312A, B, C (Styrene in SBR Rubber)
    Industry developed methods.  EMC does not provide technical support.

    Method 313A, B (Styrene in PBR Rubber)
    Industry developed methods.  EMC does not provide technical support.

    Method 315 (methylene chloride extractable organic matter)

    • Ned Shappley             919/541-7903 - Primary

    Method 316 (formaldehyde colorimetric method)
    Industry developed method.  EMC does not provide technical support.

    Method 318 (extractive FTIR method specific to mineral wool/wool fiberglass industry)

    • Dave Nash                    919/541-9425 - Primary

    Method 319 (filter efficiency; paint over-spray)
    Industry developed method.  EMC does not provide technical support.

    Method 320 (FTIR Extractive Method for any source category)

    • Dave Nash                     919/541-9425 - Primary

    Method 321 (extractive FTIR Method for Portland Cement Kiln industry)

    • Dave Nash                    919/541-9425 - Primary

    Method 323 (Formaldehyde Using Derivatization)

    • Dave Nash                     919/541-9425 - Primary

    Method 325A (VOC from Fugitive and Area Sources:  Sampler Deployment and Sample Collection)

    • David Berkowitz          919/541-4767  – Primary
    • Ned Shappley              919/541-7903- Backup

    Method 325B (VOC from Fugitive and Area Sources:  Sample Preparation and Analysis)

    • David Berkowitz          919/541-4767  – Primary
    • Ned Shappley              919/541-7903- Backup

    Method 326 Method for Determination of Isocyanates in Stationary Source Emissions

    • Ned Shappley              919/541-7903 - Primary
    • Dave Nash                     919/541-9425 - Backup

    Method 327 - Fugitive and Area Source Measurement of Selected Volatile Organic Hazardous Air Pollutants Using Specially Prepared Canisters

    • David Berkowitz          919/541-4767  – Primary
    • Ned Shappley              919/541-7903- Backup

    Top of Page

    Other Methods

    ASTM Methods

    • Ned Shappley             919/541-7903 – Primary

    SW-846 Methods

    • Click on 'SW-846 Frequent Questions' at www.epa.gov/hw-SW846
    • Click on 'Contact Us'

    Asbestos Methods

    • Kim Garnett               919/541-1158 - Primary

    Top of Page

    Criteria Pollutants

    Hydrogen Chloride (HCl)
    (see NSPS Methods 26 and 26A)

    • Ned Shappley             919/541-7903 – Primary

    Nitrogen Oxide (NOX)
    (see NSPS Methods 7, 7A, 7B, 7C, 7D, 7E, and 20)

    SO2 Interference (Method 7 and 7A)

    • Steffan Johnson         919/541-4790 - Primary

    Particulate Methods
    (see NSPS Methods 5, 5A, 5B, 5C, 5D, 5E, 5F, 5G, 5H and 17)

    • Walter Lin                  919/541-1341 - Primary

    Sulfur Dioxide (SO2)
    (see NSPS Methods 6, 6A, 6B, 6C, and 8)

    SO2/NOx/CO2 Method

    • Walter Lin                  919/541-1341 - Primary
    • Kim Garnett               919/541-1158 - Backup

    Top of Page

    Organic And Toxic Pollutant Methods

    Ammonia

    • Dave Nash                     919/541-9425– Primary
    • Paul Van Rooy                919-541-4464-Backup

    Urea/Ammonia

    • Dave Nash                     919/541-9425– Primary
    • Paul Van Rooy                919-541-4464-Backup

    Chromium    

    • David Berkowitz     919-541-4767 – Primary

    Mercury

    • Ned Shappley             919/541-7903 - Primary

    Multiple Metals

    • Kim Garnett                  919/541-1158 – Primary                          

    Organic Compounds
    see NSPS Methods 18, 21, 23, 24, 24A, 25, 25A, 25B, and 27)

    Dioxin/Furan
    (see NSPS Method 23)

    • Ned Shappley             919/541-7903 - Primary
    • Hannah Halliday         919/541-2431 - Backup

    Hazardous Air Pollutants       

    • Ned Shappley             919/541-7903 - Primary
    • Paul Van Rooy            919/541-4464 - Backup
    • Hannah Halliday         919/541-2431 - Backup

    Volatile Organic Compounds
    (see NSPS Methods 18, 21, 23, 24, 24A, 25, 25A, 25B, and 27)

    Volatile Organic Test Methods

    • Ned Shappley                   919/541-7903 – Primary
    • David Berkowitz               919-541-4767 – Backup
    • Hannah Halliday              919/541-2431 - Backup

    Methane Measurements

    • Ned Shappley             919/541-7903 – Primary
    • Paul Van Rooy            919/541-4464 - Backup
    • Hannah Halliday         919/541-2431 – Backup

    Top of Page

    Specialty Methods

    Calibration Orifices

    • Kim Garnett                  919/541-1158 - Primary

    FTIR (open path)

    • Dave Nash                    919/541-9425 - Primary

    FTIR (stack)

    • Dave Nash                     919/541-9425 - Primary

    Landfill Test Methods

    • Dave Nash                     919/541-9425 – Primary

    3-D Pitot             

    • Walter Lin                919/541-1341 – Primary

    Leak Detection

    • Ned Shappley             919/541-7903 – Primary
    • Dave Nash                     919/541-9425 – Backup

    Top of Page

    Continuous Emission Measurement Systems (CEMS)

    40 CFR Part 60 - NSPS
    Performance Specification 1

    • Kim Garnett             919/541-1158 - Primary

    Performance Specification 2/Procedure 1

    • Kim Garnett             919/541-1158 - Primary

    Performance Specification 3/Procedure 1

    • Kim Garnett             919/541-1158 - Primary

    Performance Specification 4/Procedure 1

    • Kim Garnett             919/541-1158 - Primary

    Performance Specification 4A/Procedure 1

    • Kim Garnett             919/541-1158 - Primary

    Performance Specification 4B/Procedure 1

    • Kim Garnett             919/541-1158 - Primary

    Performance Specification 5

    • Kim Garnett             919/541-1158 - Primary
    • David Berkowitz     919-541-4767 – Backup

    Performance Specification 6

    • Kim Garnett             919/541-1158 - Primary

    Performance Specification 7

    • Kim Garnett             919/541-1158 - Primary

    Performance Specification 8

    • Ned Shappley             919/541-7903 - Primary 

    Performance Specification 8A

    • Ned Shappley             919/541-7903 - Primary

    Performance Specification 9

    • David Berkowitz     919-541-4767 3 - Primary

    Performance Specification 11/Procedure 2

    • Kim Garnett                 919/541-1158 - Primary

    Performance Specification 12A/Procedure 5

    • Ned Shappley             919/541-7903 - Primary

    Performance Specification 12B/Procedure 5      

    • Ned Shappley             919/541-7903 - Primary

    Performance Specification 15

    • Dave Nash                     919/541-9425 - Primary

    Performance Specification 16

    • Kim Garnett                 919/541-1158 - Primary

    Performance Specification 18/Procedure 6

    • Kim Garnett                 919/541-1158 – Primary
    • Walter Lin                     919/541-1341 – Back-up

    Performance Specification 19/Procedure 7

    • Ned Shappley              919/541-7903- Primary
    • David Berkowitz          919/541-4767  – Backup

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